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Determination of dihydrocapsaicin adulteration in dietary supplements using LC-MS/MS

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dc.contributor.authorDİNCEL, DEMET
dc.contributor.authorOlgan, Hatice
dc.contributor.authorCanbaloglu, Zeynep
dc.contributor.authorYalcin, Sule
dc.contributor.authorErkucuk, Aysen
dc.contributor.authorTIRIS, GİZEM
dc.contributor.authorGÖREN, AHMET CEYHAN
dc.contributor.institutionauthorDİNCEL, DEMET
dc.contributor.institutionauthorTIRIS, GİZEM
dc.contributor.institutionauthorGÖREN, AHMET CEYHAN
dc.date.accessioned2020-09-03T20:59:08Z
dc.date.available2020-09-03T20:59:08Z
dc.date.issued2020-01-01T00:00:00Z
dc.description.abstractAdulterations of dietary supplements are serious threats to public health in all around of world. Nowadays, in order to obtain the intended effect from natural remedies, the adulteration of natural products via artificial or harmful chemicals are increasing. A rapid LC-MS/MS method for determination of capsaicin and dihydrocapsaicin in dietary supplements via Fortis C18 (150 x 3 mm; 3 mu m) column at 25 degrees C was developed and validated in a mixture of mobile phase A (1 % formic acid solution and 0.1 % ammonium formate in water) and B (1 % formic acid solution and 0.1 % ammonium formate in methanol) with gradient program at a flow rate of 0.35 mL/min. The recoveries of developed methods weytre obtained in the range of % 95.4-106.3 for capsaicin and % 96.3-108.9 for dihydrocapsaicin. This study shows that synthetic compound dihydrocapsaicin is widely use in dietary supplements products for adulteration to increase the effects of product without any declaration.
dc.identifier.citationDİNCEL D., Olgan H., Canbaloglu Z., Yalcin S., Erkucuk A., TIRIS G., GÖREN A. C. , -Determination of dihydrocapsaicin adulteration in dietary supplements using LC-MS/MS-, JOURNAL OF CHEMICAL METROLOGY, cilt.14, ss.77-82, 2020
dc.identifier.doi10.25135/jcm.36.20.01.1532
dc.identifier.trdizindoi.org/10.25135/jcm.36.20.01.1532
dc.identifier.trdizintrdizin
dc.identifier.urihttp://hdl.handle.net/20.500.12645/18596
dc.identifier.wosWOS:000560662700009
dc.titleDetermination of dihydrocapsaicin adulteration in dietary supplements using LC-MS/MS
dc.typeArticle
dspace.entity.typePublication
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local.publication.goal03 - Sağlık ve Kaliteli Yaşam
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