Publication: The effect of neutralizing agent on the synthesis and characterization of Mn3O4 nanoparticles
dc.contributor.author | Durmus, ZEHRA | |
dc.contributor.author | Tomas, M. | |
dc.contributor.author | Baykal, A. | |
dc.contributor.author | Kavas, H. | |
dc.contributor.author | Altincekic, T. Gurkaynak | |
dc.contributor.author | Toprak, M. S. | |
dc.date.accessioned | 2020-10-29T17:19:52Z | |
dc.date.available | 2020-10-29T17:19:52Z | |
dc.date.issued | 2010-12-01T00:00:00Z | |
dc.description.abstract | We report on the synthesis of Mn3O4 nanoparticles via a two-step hydrothermal route by using Mn(CH3COO)(2) as the only starting material and TMAOH and NaOH as hydrolysing agents. XRD and FT-IR analyses confirmed the composition and structure of Mn3O4. TEM images showed that spheroid Mn3O4 nanostructures obtained by this method have average particle size of 6 and 14 nm for NaOH and TMAOH hydrolyzed samples respectively. Particle size analysis indicated a strong aggregation of nanoparticles and exhibited bi-modal distribution with average size of aggregates as similar to 250 nm and 1.1 mu m for both samples. Zeta potential analysis revealed adsorbed TMAOH species on the surface of Mn3O4 nanoparticles hydrolyzed using TMAOH. ESR analyses resulted in broader lines and smaller g values than bulk Mn3O4 nanoparticles, probably due to the exchange-coupled system with unlike spins such as canted spin at surface of high-surface-disordered nanoparticles. | |
dc.identifier.citation | Durmus Z., Tomas M., Baykal A., Kavas H., Altincekic T. G. , Toprak M. S. , -The effect of neutralizing agent on the synthesis and characterization of Mn3O4 nanoparticles-, RUSSIAN JOURNAL OF INORGANIC CHEMISTRY, cilt.55, ss.1947-1952, 2010 | |
dc.identifier.doi | 10.1134/s0036023610120211 | |
dc.identifier.scopus | 78650656399 | |
dc.identifier.uri | http://hdl.handle.net/20.500.12645/25679 | |
dc.identifier.wos | WOS:000285097100021 | |
dc.title | The effect of neutralizing agent on the synthesis and characterization of Mn3O4 nanoparticles | |
dc.type | Article | |
dspace.entity.type | Publication | |
local.avesis.id | 3cd00f84-4e5b-4b70-b421-adf590724bd0 | |
local.publication.isinternational | 1 |