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Validation of a GC-IDMS method for the metrologically traceable quantification of selected FAMEs in biodiesel

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dc.contributor.authorMORALES, Valle
dc.contributor.authorGoren, AHMET CEYHAN
dc.contributor.authorHELD, Andrea
dc.contributor.authorBILSEL, Mine
dc.contributor.authorGUNDUZ, Simay
dc.contributor.authorYILMAZ, Hasibe
dc.contributor.institutionauthorGÖREN, AHMET CEYHAN
dc.date.accessioned2020-10-29T21:53:01Z
dc.date.available2020-10-29T21:53:01Z
dc.date.issued2015-10-01T00:00:00Z
dc.description.abstractCurrent methods for the analysis of fatty acid methyl esters (FAMEs) in rapeseed oil-based biodiesel refer to operationally defined measurands, which is a practical solution for routine analysis. In this paper, a new method for the SI-traceable quantification of selected FAMEs in biodiesel and its validation are described. This method has the potential to be a reference method for applications requiring structurally defined measurands and traceability to the SI as it allows direct comparisons to well-characterised calibrants through the use of isotopically labelled analogues of the analytes as well as establishing a full uncertainty budget. The method is based on gas chromatography-isotope dilution mass spectrometry. Its performance is demonstrated through its implementation and validation in two independent laboratories and is shown to provide reliable and traceable results for selected FAMEs in biodiesel test samples.
dc.identifier.citationMORALES V., Goren A. C. , HELD A., BILSEL M., GUNDUZ S., YILMAZ H., -Validation of a GC-IDMS method for the metrologically traceable quantification of selected FAMEs in biodiesel-, ACCREDITATION AND QUALITY ASSURANCE, cilt.20, ss.411-419, 2015
dc.identifier.doi10.1007/s00769-015-1144-1
dc.identifier.scopus84942506399
dc.identifier.urihttp://hdl.handle.net/20.500.12645/26456
dc.identifier.wosWOS:000361821000010
dc.titleValidation of a GC-IDMS method for the metrologically traceable quantification of selected FAMEs in biodiesel
dc.typeArticle
dspace.entity.typePublication
local.avesis.ida177f851-54aa-4d3e-81d9-73c225b894dc
local.publication.isinternational1
relation.isAuthorOfPublication07fcea81-8515-4cd4-86f2-047fe6b2df71
relation.isAuthorOfPublication.latestForDiscovery07fcea81-8515-4cd4-86f2-047fe6b2df71
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